Chloroform-d, 99.8 atom % D, contains 1 % (v/v) TMS

Code: 151831-50G D2-231

Not available outside of the UK & Ireland.

Application

Chloroform-d has been used as the deuterated solvent for the NMR spectral studies of the corresponding chiral derivatives of β-aminopropanoic acid containing the ...


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Your Price
$50.29 50G
Discontinued

Not available outside of the UK & Ireland.

Application

Chloroform-d has been used as the deuterated solvent for the NMR spectral studies of the corresponding chiral derivatives of β-aminopropanoic acid containing the α-phenylethyl group, which serve as useful starting materials for the asymmetric synthesis of β-amino acids.

General description

Chloroform-d (Deuterochloroform, CDCl3) is a deuterated derivative of chloroform. It contains 1%(v/v) TMS (Tetramethylsilane, added as a stabilizer). Quantitative infrared spectral investigations of carbon-deuterium stretching bands of chloroform-d in various organic solvents have been reported. Raman difference spectroscopic studies of mixtures of chloroform-d and liquid chloroform have been conducted to evaluate frequency shifts in the in the ν1 and ν2 bands of CHCl3 and CDCl3.

Packaging

50, 100, 250 g in glass bottle

assay99% (CP)
bp60.9 °C (lit.)
contains1 % (v/v) TMS
density1.500 g/mL at 25 °C (lit.)
formliquid
impurities≤0.0100% waterwater
InChI keyHEDRZPFGACZZDS-MICDWDOJSA-N
InChI1S/CHCl3/c2-1(3)4/h1H/i1D
isotopic purity99.8 atom % D
mass shiftM+1
mp−64 °C (lit.)
Quality Level200
refractive indexn20/D 1.444 (lit.)
SMILES string[2H]C(Cl)(Cl)Cl
technique(s)NMR: suitable
Cas Number865-49-6
Hazard Class6.1
Un Number1888
Pack GroupIII
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