9-Phenanthrylmagnesium bromide, 0.5 M in THF

Code: 563749-50ML D2-231

Not available outside of the UK & Ireland.

Application

9-Phenanthrylmagnesium bromide can be used as a reagent to prepare: 9-alkyl and 9-arylthiophenanthrenes by reacting with alkyl or aryl thiol compounds. (S

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Your Price
$230.55 50ML

Not available outside of the UK & Ireland.

Application

9-Phenanthrylmagnesium bromide can be used as a reagent to prepare: 9-alkyl and 9-arylthiophenanthrenes by reacting with alkyl or aryl thiol compounds. (S)-α-methylbenzyl 1-(9-phenanthryl)-2-naphthoate by treating with (S)- α -methylbenzyl methoxy-2-naphthoate. 1-(9-Phenanthryl)-1-phenylethanol (carbinol) by reacting with acetophenone. The obtained carbinol undergoes dehydration reaction in the presence of acetic acid and sulfuric acid to afford 1-(9-phenanthryl)-1-phenylethene (PPE).

General description

9-phenanthrylmagnesium bromide is a Grignard reagent. It can be prepared using magnesium turnings and 9-bromophenanthrene under anhydrous condition.

Legal Information

Product of Rieke Metals, Inc. Rieke is a registered trademark of Rieke Metals, Inc.

Packaging

50 mL in Sure/Seal™

bp65 °C (lit.)
concentration0.5 M in THF
density0.970 g/mL at 25 °C (lit.)
InChI keyACMUZKQPXSHTGB-UHFFFAOYSA-M
InChI1S/C14H9.BrH.Mg/c1-3-7-13-11(5-1)9-10-12-6-2-4-8-14(12)13;;/h1-9H;1H;/q;;+1/p-1
Quality Level100
reaction suitabilityreaction type: Grignard Reaction
SMILES stringBr[Mg]c1cc2ccccc2c3ccccc13
storage temp.2-8°C
Cas Number71112-64-6
Hazard Class3
Un Number2924
Pack Group2
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